Comments on: Factors deciding choice between Flame and Graphite Furnace Atomization in Atomic Absorption Spectroscopic Analysis https://lab-training.com/factors-deciding-choice-between-flame-and-graphite-furnace-atomization-in-atomic-absorption-spectroscopic-analysis/ Experience Beyond Books Sat, 27 Nov 2021 04:11:14 +0000 hourly 1 https://wordpress.org/?v=6.7.2 By: James https://lab-training.com/factors-deciding-choice-between-flame-and-graphite-furnace-atomization-in-atomic-absorption-spectroscopic-analysis/#comment-156954 Sat, 27 Nov 2021 04:11:14 +0000 https://lab-training.com/?p=15298#comment-156954 Helpful Content Sir, Graphite Furnace disturbing me, before reaching out here

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By: Dr. Deepak Bhanot https://lab-training.com/factors-deciding-choice-between-flame-and-graphite-furnace-atomization-in-atomic-absorption-spectroscopic-analysis/#comment-91438 Fri, 11 May 2018 11:12:20 +0000 https://lab-training.com/?p=15298#comment-91438 In reply to Zainorain.

Choice of technique will depend on the expected concentration levels of Zinc. In case these lie in ppm range then flame version is fine. For lower concentrations you are advised graphite furnace atomization.

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By: Zainorain https://lab-training.com/factors-deciding-choice-between-flame-and-graphite-furnace-atomization-in-atomic-absorption-spectroscopic-analysis/#comment-91435 Fri, 11 May 2018 07:56:50 +0000 https://lab-training.com/?p=15298#comment-91435 Hello Sir thank you for the article. However, I have a question.

Let’s say if I want to determine the Zinc content in fruit juice, should I use flame AAS or graphite furnace AAS, and why so? Is it due to the fruit juice or to the mineral content?

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By: Dr. Deepak Bhanot https://lab-training.com/factors-deciding-choice-between-flame-and-graphite-furnace-atomization-in-atomic-absorption-spectroscopic-analysis/#comment-88552 Wed, 14 Mar 2018 05:14:37 +0000 https://lab-training.com/?p=15298#comment-88552 In reply to FABIYI ADEYINKA.

First of all check the remaining life of your hollow cathode lamps. strongly suspect that they are nearing end of shelf life. If shelf life is not over or nearing expiry see if the procedure adopted is a validated one.

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By: FABIYI ADEYINKA https://lab-training.com/factors-deciding-choice-between-flame-and-graphite-furnace-atomization-in-atomic-absorption-spectroscopic-analysis/#comment-88534 Tue, 13 Mar 2018 13:40:21 +0000 https://lab-training.com/?p=15298#comment-88534 I carried out an AAS analysis on aquatic macro-invertebrates to detect the level of heavy metals in them but most of my results in Ni, Pb, Cd and Cr came out very low while most of the result read 0.00 (ppm) except for zinc that has higher values. What could cause this?

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By: Dr. Deepak Bhanot https://lab-training.com/factors-deciding-choice-between-flame-and-graphite-furnace-atomization-in-atomic-absorption-spectroscopic-analysis/#comment-2043 Wed, 12 Feb 2014 11:44:40 +0000 https://lab-training.com/?p=15298#comment-2043 In reply to Nureni Bashiru.

Hi Nureni,
It appears that your burner head or burner is having some remaining contamination from previous analysis.Aspirate with 1% nitric acid solution for around 5 minutes and follow with same time with water.The flame should be free of the red glow.Even then if the glow remains check the purity of water as it may be having contamination of alkali/alkaline earth elements

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By: Nureni Bashiru https://lab-training.com/factors-deciding-choice-between-flame-and-graphite-furnace-atomization-in-atomic-absorption-spectroscopic-analysis/#comment-2042 Wed, 12 Feb 2014 10:03:07 +0000 https://lab-training.com/?p=15298#comment-2042 I have Thermo S-series atomic absorption spectrometer in my lab, but the flame is not coming up properly. That is, it always glow red and this is not useful for a good analysis. The air and gas were checked and they were in order.
What can I do to make it work sir. I mean, how can i troubleshoot the AAS.
Thank you sir.

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By: Dr. Deepak Bhanot https://lab-training.com/factors-deciding-choice-between-flame-and-graphite-furnace-atomization-in-atomic-absorption-spectroscopic-analysis/#comment-1782 Sat, 11 Jan 2014 09:03:37 +0000 https://lab-training.com/?p=15298#comment-1782 In reply to abdulqawi.

Hi Abdulqawi,
The sensitivitiy is dependent on the number of ground state atoms in the light path.In flame analysis you can rotate the burner or even adjust its height to get the maximum absorbance thereby giving improved sensitivity.

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By: abdulqawi https://lab-training.com/factors-deciding-choice-between-flame-and-graphite-furnace-atomization-in-atomic-absorption-spectroscopic-analysis/#comment-1781 Sat, 11 Jan 2014 07:16:05 +0000 https://lab-training.com/?p=15298#comment-1781 how can to adjust the flame of aceylye gas and nitrouse gas to get goog reading

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